Note: A different textbook was used last year. Some material on this exam may not have been covered yet.

 

EXAM 1

CHEMISTRY 220

Friday, September 27, 1996

 

NAME (print): ___________________________________________________

 

TA:_____________________ Day:_________________ Time:__________

 

Take a few moments to look over the exam. Answer each question on the exam paper.

 

Do all preliminary drawing or computation in a blue book.

 

Blue books will not be collected.

 

The exam is 55 minutes.

 

The points should be an indication of the time required for solution.

 

STOP writing when you are asked to do so.

 

REMEMBER: Neatness is to your advantage.

 

1. (15 pts) ______

 

 

2. (22 pts) ______

 

 

3. (20 pts) ______

 

 

4. (9 pts) ______

 

 

5. (15 pts) ______

 

 

6. (10 pts) ______

 

 

7. (9 pts) ______

________________________________

 

Total (100 pts)

 

1. (15 pts) A problem on conformational analysis.

 

a) (6 pts) Draw Newman projections of propane for the most and least stable

conformations. Label which one is which. In a single word, describe each diagram.

 

 

b) (5 pts) Draw a potential energy diagram (energy vs. angle of rotation) for rotation about a

C-C bond of propane.

 

c) (4 pts) Using the following values, calculate (show work) the barrier to rotation about a

C-C bond of propane: H/H, eclipsed, 1.0 kcal/mol; CH3/H eclipsed, 1.4 kcal/mol;

CH3/CH3, eclipsed, 2.5 kcal/mol; CH3/CH3, gauche, 0.9 kcal/mol. Briefly explain

your reasoning. Locate this barrier in the diagram of part b.

 

2. (22 pts) On the structure of acrylonitrile.

 

a) (4 pts) Acrylonitrile (1) is used to make polymers. Redraw 1 using lines for bonds to

reflect the true geometry of acrylonitrile (be faithful to bond angles; ignore the

numbers). In a single word, how would best describe the shape of acrylonitrile (think

of the shapes of ethane, ethylene, and acetylene)?

 

b) (6 pts) Rather than using lines for bonds, use an orbital (e. g., sp3, 1s, p) picture to

illustrate the structure of acrylonitrile. Label one of each hybrid orbital. Note: Only use

the large lobe of hybrid orbitals to make your picture clear.

 

c) (3 pts) How many s-bonds are in 1?

 

d) (3 pts) How many p-bonds are in 1?

 

e) (3 pts) What is the value (degrees) of the bond angle C3-C5-N6?

 

f) (3 pts) What is the value (degrees) of the dihedral angle H1-C2-C3-H4?

 

3. (20 pts) Tertiary-butyl alcohol 1 has a pKa of 18 while acetone 2, has a pKa of 20.

Answer the following questions regarding this equilibrium.

 

a) (3 pts) Circle the conjugate base of acetone.

 

b) (3 pts) What is the principal factor that makes the C-H bond of acetone about 1030

times more acidic than methane?

 

c) (3 pts) Place a square around the strongest acid.

 

d) (3 pts) Place equilibrium arrows in the rectangle to illustrate clearly the direction of

the equilibrium.

 

e) (3 pts) What is the value for Keq of the reaction shown?

 

Keq=

 

f) (5 pts) What is the value (show work) of DGoeq at 27 oC: R = 2.0 x 10-3 kcal/mol-

oK [DGo = -RT lnKeq]?

 

DGoeq=

 

4. (a: 3 pts; b: 3 pts; c: 3 pts = 9 pts) All reactions must balance atoms and charges. Use

curved arrows for electron flow and complete or correct the following reactions by

supplying the missing information. Include charges where necessary.

 

 

5. (5 x 3 pts = 15 pts) Of ethylene, ethane, and acetylene, which one satisfies the following

criteria best.

 

 

a) The carbon-carbon bond with the lowest rotational barrier.

 

 

 

b) The largest C-H bond dissociation energy.

 

 

 

c) The shortest C-H bond.

 

 

 

d) The most acidic C-H bond.

 

 

 

e) A carbon-carbon bond length of 1.33Å.

 

 

 

6. (5 x 2 pts = 10 pts) In 1832, Liebig and Wöhler jointly published a paper on the benzoyl

radical, C7H5O. In those days, a radical was considered to be a group that could not be

altered. They prepared a number of derivatives of the benzoyl radical, changing the X

group in structure 1. For each of the following X groups, name the functional group that

is attached to the benzene ring (i. e.; RCOX).

a) X=Cl

 

b) X=OR

 

c) X=NH2

 

d) X=R

 

e) X= RCO2 (attached at oxygen)

 

 

7. (3 x 3 pts =9 pts) Potpourri

 

a) Arrange the following in order of electron affinity: Methyl radical, fluorine atom, and

hydroxyl radical.

 

 

> >

 

 

b) Arrange the following in order of pKa: Cl3CCO2H, CH4, H2O, and CH3CO2H.

 

 

< < <

 

 

c) Arrange the following in order of boiling point: 2,2-dimethylpropane, n-pentane and

hexane.

 

 

< <